In-situ and operando catalysis techniques have revolutionized the way researchers study catalytic processes by enabling real-time monitoring of catalysts under reaction conditions. In-situ catalysis refers to the analysis of catalysts in their active state within the reaction environment, allowing for a more accurate representation of catalytic behavior compared to traditional ex-situ techniques, where catalysts are isolated from the reaction. By capturing data in real time, researchers can gain insights into the catalyst's structural, electronic, and chemical changes during the reaction process, providing a more holistic understanding of catalyst performance. Operando catalysis, which involves monitoring both the catalyst and the reaction simultaneously under realistic operating conditions, takes this a step further. This approach allows for the observation of dynamic changes in catalyst morphology, electronic properties, and reaction intermediates as the reaction progresses.
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